Abstract

We demonstrate fiber mode-locked dual-frequency comb spectroscopy for broadband, high-resolution measurements in a rapid compression machine (RCM). We apply an apodization technique to improve the short-term signal-to-noise-ratio (SNR), which enables broadband spectroscopy at combustion-relevant timescales. We measure the absorption on 24345 individual wavelength elements (comb teeth) between 5967 and 6133 cm−1 at 704 µs time resolution during a 12 ms compression of a CH4-N2 mixture. We discuss the effect of the apodization technique on the absorption spectra, and apply an identical effect to the spectral model during fitting to recover the mixture temperature. The fitted temperature is compared against an adiabatic model, and found to be in good agreement with expected trends. This work demonstrates the potential of DCS to be used as an in situ diagnostic tool for broadband, high-resolution measurements in engine-like environments.

© 2019 Optical Society of America under the terms of the OSA Open Access Publishing Agreement

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2018 (2)

2017 (9)

P. J. Schroeder, R. J. Wright, S. Coburn, B. Sodergren, K. C. Cossel, S. Droste, G. W. Truong, E. Baumann, F. R. Giorgetta, I. Coddington, N. R. Newbury, and G. B. Rieker, “Dual frequency comb laser absorption spectroscopy in a 16 MW gas turbine exhaust,” Proc. Combust. Inst. 36(3), 4565–4573 (2017).
[Crossref]

C. Dumitrache, M. Baumgardner, A. Boissiere, A. Maria, J. Roucis, A. J. Marchese, and A. Yalin, “A study of laser induced ignition of methane–air mixtures inside a Rapid Compression Machine,” Proc. Combust. Inst. 36(3), 3431–3439 (2017).
[Crossref]

P. J. Schroeder, D. J. Pfotenhauer, J. Yang, F. R. Giorgetta, W. C. Swann, I. Coddington, N. R. Newbury, and G. B. Rieker, “High temperature comparison of the HITRAN2012 and HITEMP2010 water vapor absorption databases to frequency comb measurements,” J. Quant. Spectrosc. Radiat. Transf. 203, 194–205 (2017).
[Crossref]

I. E. Gordon, L. S. Rothman, C. Hill, R. V. Kochanov, Y. Tan, P. F. Bernath, M. Birk, V. Boudon, A. Campargue, K. V. Chance, B. J. Drouin, J.-M. Flaud, R. R. Gamache, J. T. Hodges, D. Jacquemart, V. I. Perevalov, A. Perrin, K. P. Shine, M.-A. H. Smith, J. Tennyson, G. C. Toon, H. Tran, V. G. Tyuterev, A. Barbe, A. G. Császár, V. M. Devi, T. Furtenbacher, J. J. Harrison, J.-M. Hartmann, A. Jolly, T. J. Johnson, T. Karman, I. Kleiner, A. A. Kyuberis, J. Loos, O. M. Lyulin, S. T. Massie, S. N. Mikhailenko, N. Moazzen-Ahmadi, H. S. P. Müller, O. V. Naumenko, A. V. Nikitin, O. L. Polyansky, M. Rey, M. Rotger, S. W. Sharpe, K. Sung, E. Starikova, S. A. Tashkun, J. V. Auwera, G. Wagner, J. Wilzewski, P. Wcisło, S. Yu, and E. J. Zak, “The HITRAN2016 molecular spectroscopic database,” J. Quant. Spectrosc. Radiat. Transf. 203, 3–69 (2017).
[Crossref]

O. Kara, L. Maidment, T. Gardiner, P. G. Schunemann, and D. T. Reid, “Dual-comb spectroscopy in the spectral fingerprint region using OPGaP optical parametric oscillators,” Opt. Express 25(26), 32713–32721 (2017).
[Crossref]

E. F. Nasir and A. Farooq, “Time-resolved temperature measurements in a rapid compression machine using quantum cascade laser absorption in the intrapulse mode,” Proc. Combust. Inst. 36(3), 4453–4460 (2017).
[Crossref]

T. Werblinski, P. Fendt, L. Zigan, and S. Will, “High-speed combustion diagnostics in a rapid compression machine by broadband supercontinuum absorption spectroscopy,” Appl. Opt. 56(15), 4443–4453 (2017).
[Crossref] [PubMed]

C. S. Goldenstein, R. M. Spearrin, J. B. Jeffries, and R. K. Hanson, “Infrared laser-absorption sensing for combustion gases,” Pror. Energy Combust. Sci. 60, 132–176 (2017).
[Crossref]

S. S. Goldsborough, S. Hochgreb, G. Vanhove, M. S. Wooldridge, H. J. Curran, and C.-J. Sung, “Advances in rapid compression machine studies of low- and intermediate-temperature autoignition phenomena,” Pror. Energy Combust. Sci. 63(Supplement C), 1–78 (2017).
[Crossref]

2016 (4)

2015 (2)

2014 (3)

T. Ideguchi, A. Poisson, G. Guelachvili, N. Picqué, and T. W. Hänsch, “Adaptive real-time dual-comb spectroscopy,” Nat. Commun. 5(1), 3375 (2014).
[Crossref] [PubMed]

G. Villares, A. Hugi, S. Blaser, and J. Faist, “Dual-comb spectroscopy based on quantum-cascade-laser frequency combs,” Nat. Commun. 5(1), 5192 (2014).
[Crossref] [PubMed]

D. A. Long, A. J. Fleisher, K. O. Douglass, S. E. Maxwell, K. Bielska, J. T. Hodges, and D. F. Plusquellic, “Multiheterodyne spectroscopy with optical frequency combs generated from a continuous-wave laser,” Opt. Lett. 39(9), 2688–2690 (2014).
[Crossref] [PubMed]

2012 (1)

2011 (1)

E. Baumann, F. R. Giorgetta, W. C. Swann, A. M. Zolot, I. Coddington, and N. R. Newbury, “Spectroscopy of the methane ν 3 band with an accurate midinfrared coherent dual-comb spectrometer,” Phys. Rev. A 84(6), 062513 (2011).
[Crossref]

2010 (2)

N. R. Newbury, I. Coddington, and W. Swann, “Sensitivity of coherent dual-comb spectroscopy,” Opt. Express 18(8), 7929–7945 (2010).
[Crossref] [PubMed]

I. Coddington, W. C. Swann, and N. R. Newbury, “Coherent dual-comb spectroscopy at high signal-to-noise ratio,” Phys. Rev. A 82(4), 043817 (2010).
[Crossref]

2007 (1)

C. L. Hagen and S. T. Sanders, “Investigation of multi-species (H 2 O 2 and H 2 O) sensing and thermometry in an HCCI engine by wavelength-agile absorption spectroscopy,” Meas. Sci. Technol. 18(7), 1992–1998 (2007).
[Crossref]

2006 (2)

G. Mittal and C.-J. Sung, “Aerodynamics inside a rapid compression machine,” Combust. Flame 145(1), 160–180 (2006).
[Crossref]

J. L. Hall, “Nobel Lecture: Defining and measuring optical frequencies,” Rev. Mod. Phys. 78(4), 1279–1295 (2006).
[Crossref] [PubMed]

2005 (2)

A. Schliesser, M. Brehm, F. Keilmann, and D. van der Weide, “Frequency-comb infrared spectrometer for rapid, remote chemical sensing,” Opt. Express 13(22), 9029–9038 (2005).
[Crossref] [PubMed]

L. A. Kranendonk, J. W. Walewski, T. Kim, and S. T. Sanders, “Wavelength-agile sensor applied for HCCI engine measurements,” Proc. Combust. Inst. 30(1), 1619–1627 (2005).
[Crossref]

2004 (1)

2001 (1)

1972 (1)

T. Kobayashi, T. Sueta, Y. Cho, and Y. Matsuo, “High‐repetition‐rate optical pulse generator using a Fabry‐Perot electro‐optic modulator,” Appl. Phys. Lett. 21(8), 341–343 (1972).
[Crossref]

Alden, C. B.

Auwera, J. V.

I. E. Gordon, L. S. Rothman, C. Hill, R. V. Kochanov, Y. Tan, P. F. Bernath, M. Birk, V. Boudon, A. Campargue, K. V. Chance, B. J. Drouin, J.-M. Flaud, R. R. Gamache, J. T. Hodges, D. Jacquemart, V. I. Perevalov, A. Perrin, K. P. Shine, M.-A. H. Smith, J. Tennyson, G. C. Toon, H. Tran, V. G. Tyuterev, A. Barbe, A. G. Császár, V. M. Devi, T. Furtenbacher, J. J. Harrison, J.-M. Hartmann, A. Jolly, T. J. Johnson, T. Karman, I. Kleiner, A. A. Kyuberis, J. Loos, O. M. Lyulin, S. T. Massie, S. N. Mikhailenko, N. Moazzen-Ahmadi, H. S. P. Müller, O. V. Naumenko, A. V. Nikitin, O. L. Polyansky, M. Rey, M. Rotger, S. W. Sharpe, K. Sung, E. Starikova, S. A. Tashkun, J. V. Auwera, G. Wagner, J. Wilzewski, P. Wcisło, S. Yu, and E. J. Zak, “The HITRAN2016 molecular spectroscopic database,” J. Quant. Spectrosc. Radiat. Transf. 203, 3–69 (2017).
[Crossref]

Barbe, A.

I. E. Gordon, L. S. Rothman, C. Hill, R. V. Kochanov, Y. Tan, P. F. Bernath, M. Birk, V. Boudon, A. Campargue, K. V. Chance, B. J. Drouin, J.-M. Flaud, R. R. Gamache, J. T. Hodges, D. Jacquemart, V. I. Perevalov, A. Perrin, K. P. Shine, M.-A. H. Smith, J. Tennyson, G. C. Toon, H. Tran, V. G. Tyuterev, A. Barbe, A. G. Császár, V. M. Devi, T. Furtenbacher, J. J. Harrison, J.-M. Hartmann, A. Jolly, T. J. Johnson, T. Karman, I. Kleiner, A. A. Kyuberis, J. Loos, O. M. Lyulin, S. T. Massie, S. N. Mikhailenko, N. Moazzen-Ahmadi, H. S. P. Müller, O. V. Naumenko, A. V. Nikitin, O. L. Polyansky, M. Rey, M. Rotger, S. W. Sharpe, K. Sung, E. Starikova, S. A. Tashkun, J. V. Auwera, G. Wagner, J. Wilzewski, P. Wcisło, S. Yu, and E. J. Zak, “The HITRAN2016 molecular spectroscopic database,” J. Quant. Spectrosc. Radiat. Transf. 203, 3–69 (2017).
[Crossref]

Baumann, E.

S. Coburn, C. B. Alden, R. Wright, K. Cossel, E. Baumann, G.-W. Truong, F. Giorgetta, C. Sweeney, N. R. Newbury, K. Prasad, I. Coddington, and G. B. Rieker, “Regional trace-gas source attribution using a field-deployed dual frequency comb spectrometer,” Optica 5(4), 320–327 (2018).
[Crossref]

P. J. Schroeder, R. J. Wright, S. Coburn, B. Sodergren, K. C. Cossel, S. Droste, G. W. Truong, E. Baumann, F. R. Giorgetta, I. Coddington, N. R. Newbury, and G. B. Rieker, “Dual frequency comb laser absorption spectroscopy in a 16 MW gas turbine exhaust,” Proc. Combust. Inst. 36(3), 4565–4573 (2017).
[Crossref]

G.-W. Truong, E. M. Waxman, K. C. Cossel, E. Baumann, A. Klose, F. R. Giorgetta, W. C. Swann, N. R. Newbury, and I. Coddington, “Accurate frequency referencing for fieldable dual-comb spectroscopy,” Opt. Express 24(26), 30495–30504 (2016).
[Crossref] [PubMed]

E. Baumann, F. R. Giorgetta, W. C. Swann, A. M. Zolot, I. Coddington, and N. R. Newbury, “Spectroscopy of the methane ν 3 band with an accurate midinfrared coherent dual-comb spectrometer,” Phys. Rev. A 84(6), 062513 (2011).
[Crossref]

Baumgardner, M.

C. Dumitrache, M. Baumgardner, A. Boissiere, A. Maria, J. Roucis, A. J. Marchese, and A. Yalin, “A study of laser induced ignition of methane–air mixtures inside a Rapid Compression Machine,” Proc. Combust. Inst. 36(3), 3431–3439 (2017).
[Crossref]

Bernath, P. F.

I. E. Gordon, L. S. Rothman, C. Hill, R. V. Kochanov, Y. Tan, P. F. Bernath, M. Birk, V. Boudon, A. Campargue, K. V. Chance, B. J. Drouin, J.-M. Flaud, R. R. Gamache, J. T. Hodges, D. Jacquemart, V. I. Perevalov, A. Perrin, K. P. Shine, M.-A. H. Smith, J. Tennyson, G. C. Toon, H. Tran, V. G. Tyuterev, A. Barbe, A. G. Császár, V. M. Devi, T. Furtenbacher, J. J. Harrison, J.-M. Hartmann, A. Jolly, T. J. Johnson, T. Karman, I. Kleiner, A. A. Kyuberis, J. Loos, O. M. Lyulin, S. T. Massie, S. N. Mikhailenko, N. Moazzen-Ahmadi, H. S. P. Müller, O. V. Naumenko, A. V. Nikitin, O. L. Polyansky, M. Rey, M. Rotger, S. W. Sharpe, K. Sung, E. Starikova, S. A. Tashkun, J. V. Auwera, G. Wagner, J. Wilzewski, P. Wcisło, S. Yu, and E. J. Zak, “The HITRAN2016 molecular spectroscopic database,” J. Quant. Spectrosc. Radiat. Transf. 203, 3–69 (2017).
[Crossref]

Bielska, K.

Birk, M.

I. E. Gordon, L. S. Rothman, C. Hill, R. V. Kochanov, Y. Tan, P. F. Bernath, M. Birk, V. Boudon, A. Campargue, K. V. Chance, B. J. Drouin, J.-M. Flaud, R. R. Gamache, J. T. Hodges, D. Jacquemart, V. I. Perevalov, A. Perrin, K. P. Shine, M.-A. H. Smith, J. Tennyson, G. C. Toon, H. Tran, V. G. Tyuterev, A. Barbe, A. G. Császár, V. M. Devi, T. Furtenbacher, J. J. Harrison, J.-M. Hartmann, A. Jolly, T. J. Johnson, T. Karman, I. Kleiner, A. A. Kyuberis, J. Loos, O. M. Lyulin, S. T. Massie, S. N. Mikhailenko, N. Moazzen-Ahmadi, H. S. P. Müller, O. V. Naumenko, A. V. Nikitin, O. L. Polyansky, M. Rey, M. Rotger, S. W. Sharpe, K. Sung, E. Starikova, S. A. Tashkun, J. V. Auwera, G. Wagner, J. Wilzewski, P. Wcisło, S. Yu, and E. J. Zak, “The HITRAN2016 molecular spectroscopic database,” J. Quant. Spectrosc. Radiat. Transf. 203, 3–69 (2017).
[Crossref]

Blaser, S.

G. Villares, A. Hugi, S. Blaser, and J. Faist, “Dual-comb spectroscopy based on quantum-cascade-laser frequency combs,” Nat. Commun. 5(1), 5192 (2014).
[Crossref] [PubMed]

Boissiere, A.

C. Dumitrache, M. Baumgardner, A. Boissiere, A. Maria, J. Roucis, A. J. Marchese, and A. Yalin, “A study of laser induced ignition of methane–air mixtures inside a Rapid Compression Machine,” Proc. Combust. Inst. 36(3), 3431–3439 (2017).
[Crossref]

Boudon, V.

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P. J. Schroeder, D. J. Pfotenhauer, J. Yang, F. R. Giorgetta, W. C. Swann, I. Coddington, N. R. Newbury, and G. B. Rieker, “High temperature comparison of the HITRAN2012 and HITEMP2010 water vapor absorption databases to frequency comb measurements,” J. Quant. Spectrosc. Radiat. Transf. 203, 194–205 (2017).
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F. C. Cruz, D. L. Maser, T. Johnson, G. Ycas, A. Klose, F. R. Giorgetta, I. Coddington, and S. A. Diddams, “Mid-infrared optical frequency combs based on difference frequency generation for molecular spectroscopy,” Opt. Express 23(20), 26814–26824 (2015).
[Crossref] [PubMed]

E. Baumann, F. R. Giorgetta, W. C. Swann, A. M. Zolot, I. Coddington, and N. R. Newbury, “Spectroscopy of the methane ν 3 band with an accurate midinfrared coherent dual-comb spectrometer,” Phys. Rev. A 84(6), 062513 (2011).
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Massie, S. T.

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Metcalf, A. J.

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Swann, W. C.

P. J. Schroeder, D. J. Pfotenhauer, J. Yang, F. R. Giorgetta, W. C. Swann, I. Coddington, N. R. Newbury, and G. B. Rieker, “High temperature comparison of the HITRAN2012 and HITEMP2010 water vapor absorption databases to frequency comb measurements,” J. Quant. Spectrosc. Radiat. Transf. 203, 194–205 (2017).
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E. Baumann, F. R. Giorgetta, W. C. Swann, A. M. Zolot, I. Coddington, and N. R. Newbury, “Spectroscopy of the methane ν 3 band with an accurate midinfrared coherent dual-comb spectrometer,” Phys. Rev. A 84(6), 062513 (2011).
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I. Coddington, W. C. Swann, and N. R. Newbury, “Coherent dual-comb spectroscopy at high signal-to-noise ratio,” Phys. Rev. A 82(4), 043817 (2010).
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Tyuterev, V. G.

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R. V. Kochanov, I. E. Gordon, L. S. Rothman, P. Wcisło, C. Hill, and J. S. Wilzewski, “HITRAN Application Programming Interface (HAPI): A comprehensive approach to working with spectroscopic data,” J. Quant. Spectrosc. Radiat. Transf. 177, 15–30 (2016).
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C. Dumitrache, M. Baumgardner, A. Boissiere, A. Maria, J. Roucis, A. J. Marchese, and A. Yalin, “A study of laser induced ignition of methane–air mixtures inside a Rapid Compression Machine,” Proc. Combust. Inst. 36(3), 3431–3439 (2017).
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[Crossref]

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[Crossref]

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Figures (5)

Fig. 1
Fig. 1 Diagram showing the time and frequency domain representation of dual frequency comb spectroscopy. (a) Effective time domain schematic of femtosecond comb pulses originating from combs with different repetition rates, where the pulses of one comb “step through” the pulses of the other comb. The signal comb is shown in dashed red and the local oscillator comb in blue. (b) The time domain signal as recorded by the photodetector is a cross-correlation of the comb pulses – an interferogram – formed in laboratory time and with a “centerburst” when the pulses of the two combs are overlapping. (c) The comb teeth of the two combs represented in the optical frequency domain. The two comb repetition rates are fixed such that a unique heterodyne beat in the RF-domain is formed from pairs of comb teeth. (d) Individual comb teeth are resolved in the RF-domain by taking the Fourier Transform of the interferogram shown in (b).
Fig. 2
Fig. 2 Measured CO absorption feature near 6297.5 cm−1, with the same apodization applied to the measured interferogram (red) and the model (blue). The instrument line shape from apodization is apparent, but is well captured by the model. This data was coherently averaged for a period of 10 minutes to increase the signal to noise ratio and emphasize the effect of the added instrument line shape.
Fig. 3
Fig. 3 Schematic of experimental setup. The mobile DCS supplies light via single-mode fiber to a collimator, which transmits the light through the RCM combustion chamber, and is then received through a convex focusing lens onto a fast photodetector. The resulting signal is low-pass filtered before being collected with the data acquisition system. The spectrometer also provides a clock signal to the data acquisition, and the RCM start switch is linked to enable synchronous collection.
Fig. 4
Fig. 4 Measured absorbance spectra at 1 bar and 294 K with 704 μs time resolution just prior to the compression. The red traces are the unapodized data and the black traces are apodized. (a) Interferogram with both the laboratory and effective timescales shown, (b) Zoomed CH4 absorption feature for the region indicated on panel c, and (c) Full measured spectrum.
Fig. 5
Fig. 5 DCS-measured temperature from broadband fitting of the apodized spectra (purple). The red trace is the adiabatic temperature calculated using GASEQ, while the gray represents the residual percent error.

Equations (2)

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ln( P(t) P 0 )= T 0 T(t) γ γ1 dT T
f(ν)=2 Δ E sinc( 2π Δ E ν )

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