Compound formation in supported heterogeneous catalysts is an area of significant interest. In the present study, Al(ReO<sub>4</sub>)<sub>3</sub> was prepared and characterized by x-ray photoelectron spectroscopy and laser Raman spectroscopy. Characteristic spectra Al(ReO<sub>4</sub>)<sub>3</sub> for are shown and compared to several rhenium reference compounds. The reduction behavior of Al(ReO<sub>4</sub>)<sub>3</sub> is also explored; it was completely reduced to elemental rhenium in H<sub>2</sub> at 500°C.

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